C₂₇H₃₄F₄N₂O₇S

Base Information

Chemical Name:C₂₇H₃₄F₄N₂O₇S
CAS No.:1204343-95-2
Molecular Formula:C₂₇H₃₄F₄N₂O₇S
Molecular Weight:606.636
Hs Code.:

C<sub>27</sub>H<sub>34</sub>F<sub>4</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:

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Chemical Property of C₂₇H₃₄F₄N₂O₇S

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Technology Process of C₂₇H₃₄F₄N₂O₇S

There total 12 articles about C₂₇H₃₄F₄N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204343-82-7
(3R,4S,5S)-3-amino-5-(3,5-difluoro-4-nitrobenzyl)-4-hydroxytetrahydro-2H-thiopyran 1,1-dioxide hydrochloride

: 1204343-95-2
C₂₇H₃₄F₄N₂O₇S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / methanol; dichloromethane / 0.5 h / 25 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

1.3: 0.25 h / Inert atmosphere

2.1: potassium hydroxide / tetrahydrofuran / 0.33 h / Microwave irradiation

With sodium acetate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm300069y

Reference yield:

: 1123172-88-2
3,5-difluoro-4-nitro-benzonitrile

: 1204343-95-2
C₂₇H₃₄F₄N₂O₇S

Guidance literature:: Multi-step reaction with 11 steps

1.1: thionyl chloride / 0 - 25 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 5 °C / Inert atmosphere

2.2: 0.5 h / 25 °C / Cooling with ice; Inert atmosphere

3.1: phosphorus tribromide / 24 h / 25 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 2.5 h / 25 - 30 °C / Inert atmosphere

5.1: palladium diacetate; triethylamine; triphenylphosphine / tert-butyl methyl ether / 16 h / 25 °C / Inert atmosphere

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -70 °C / Inert atmosphere

7.1: Chiralpak AD-I / ethanol; n-heptane / Inert atmosphere

8.1: potassium peroxymonosulfate / tetrahydrofuran; water / 2 h / 40 °C / Inert atmosphere

9.1: hydrogenchloride / 1,4-dioxane / 2 h / 25 °C / Inert atmosphere

10.1: sodium acetate / methanol; dichloromethane / 0.5 h / 25 °C / Inert atmosphere

10.2: 1 h / Inert atmosphere

10.3: 0.25 h / Inert atmosphere

11.1: potassium hydroxide / tetrahydrofuran / 0.33 h / Microwave irradiation

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; potassium peroxymonosulfate; sodium acetate; palladium diacetate; phosphorus tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; n-heptane; dichloromethane; tert-butyl methyl ether; water; acetone;
DOI:10.1021/jm300069y

Reference yield:

: 1123172-87-1
methyl 3,5-difluoro-4-nitrobenzoate

: 1204343-95-2
C₂₇H₃₄F₄N₂O₇S

Guidance literature:: Multi-step reaction with 10 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 5 °C / Inert atmosphere

1.2: 0.5 h / 25 °C / Cooling with ice; Inert atmosphere

2.1: phosphorus tribromide / 24 h / 25 °C / Inert atmosphere

3.1: potassium carbonate / acetone / 2.5 h / 25 - 30 °C / Inert atmosphere

4.1: palladium diacetate; triethylamine; triphenylphosphine / tert-butyl methyl ether / 16 h / 25 °C / Inert atmosphere

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -70 °C / Inert atmosphere

6.1: Chiralpak AD-I / ethanol; n-heptane / Inert atmosphere

7.1: potassium peroxymonosulfate / tetrahydrofuran; water / 2 h / 40 °C / Inert atmosphere

8.1: hydrogenchloride / 1,4-dioxane / 2 h / 25 °C / Inert atmosphere

9.1: sodium acetate / methanol; dichloromethane / 0.5 h / 25 °C / Inert atmosphere

9.2: 1 h / Inert atmosphere

9.3: 0.25 h / Inert atmosphere

10.1: potassium hydroxide / tetrahydrofuran / 0.33 h / Microwave irradiation

With hydrogenchloride; lithium aluminium tetrahydride; potassium peroxymonosulfate; sodium acetate; palladium diacetate; phosphorus tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; n-heptane; dichloromethane; tert-butyl methyl ether; water; acetone;
DOI:10.1021/jm300069y