Technology Process of C26H31N3O3S
There total 15 articles about C26H31N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 9 steps
1: 3-chloro-benzenecarboperoxoic acid / ethanol
2: ethylmagnesium bromide / diethyl ether
3: diisobutylaluminium hydride / toluene
4: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
6: Lawessons reagent; pyridine / toluene / 100 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran
8: thionyl chloride / toluene
9: N-ethyl-N,N-diisopropylamine / acetonitrile
With
Lawessons reagent; pyridine; sodium chlorite; potassium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; ethylmagnesium bromide; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran
2: thionyl chloride / toluene
3: N-ethyl-N,N-diisopropylamine / acetonitrile
With
thionyl chloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 7 steps
1: PhMe2NBr3
2: sodium diformamide
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
4: Lawessons reagent; pyridine / toluene / 100 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran
6: thionyl chloride / toluene
7: N-ethyl-N,N-diisopropylamine / acetonitrile
With
Lawessons reagent; pyridine; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067