[¹⁹F]-Gal-RGD

Base Information

Chemical Name:[¹⁹F]-Gal-RGD
CAS No.:1509923-71-0
Molecular Formula:C₃₂H₄₄FN₁₁O₁₁
Molecular Weight:776.768
Hs Code.:

Synonyms:

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Chemical Property of [¹⁹F]-Gal-RGD

Chemical Property:

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Technology Process of [¹⁹F]-Gal-RGD

There total 3 articles about [¹⁹F]-Gal-RGD which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1509923-64-1
C₁₂H₁₆⁽¹⁸⁾FN₃O₇

: 1509923-71-0
[¹⁹F]-Gal-RGD

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / 0.08 h / 60 °C / Inert atmosphere

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / ethanol; water / 60 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; sodium hydroxide; In ethanol; water;
DOI:10.1021/mp4004817

Reference yield:

: 106192-43-2
2,3,4-Tri-O-acetyl-6-O-(p-tolylsulfonyl)-β-D-galactopyranosylazid

: 1509923-71-0
[¹⁹F]-Gal-RGD

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium dihydrogenphosphate; C₂₂H₃₆N₂O₆*K⁽¹⁺⁾*⁽¹⁸⁾F^(1-) / acetonitrile; water / 0.17 h / 85 °C / Inert atmosphere

2: sodium hydroxide / 0.08 h / 60 °C / Inert atmosphere

3: sodium L-ascorbate; copper(ll) sulfate pentahydrate / ethanol; water / 60 °C

With potassium dihydrogenphosphate; copper(ll) sulfate pentahydrate; C₂₂H₃₆N₂O₆*K⁽¹⁺⁾*⁽¹⁸⁾F^(1-); potassium carbonate; sodium L-ascorbate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1021/mp4004817

Reference yield:

: 106192-39-6
α-D-galactopyranosyl azide

: 1509923-71-0
[¹⁹F]-Gal-RGD

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 0 °C

1.2: 1 h / 0 °C

2.1: potassium carbonate; potassium dihydrogenphosphate; C₂₂H₃₆N₂O₆*K⁽¹⁺⁾*⁽¹⁸⁾F^(1-) / acetonitrile; water / 0.17 h / 85 °C / Inert atmosphere

3.1: sodium hydroxide / 0.08 h / 60 °C / Inert atmosphere

4.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / ethanol; water / 60 °C

With pyridine; potassium dihydrogenphosphate; copper(ll) sulfate pentahydrate; C₂₂H₃₆N₂O₆*K⁽¹⁺⁾*⁽¹⁸⁾F^(1-); potassium carbonate; sodium L-ascorbate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1021/mp4004817