t-butyl bis(4-methylbenzyl)phosphinate

Base Information

Chemical Name:t-butyl bis(4-methylbenzyl)phosphinate
CAS No.:129529-13-1
Molecular Formula:C₂₀H₂₇O₂P
Molecular Weight:330.407
Hs Code.:

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Chemical Property of t-butyl bis(4-methylbenzyl)phosphinate

Chemical Property:

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Technology Process of t-butyl bis(4-methylbenzyl)phosphinate

There total 4 articles about t-butyl bis(4-methylbenzyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18896-84-9
bis(4-methylbenzyl)phosphinic acid

: 129529-13-1
t-butyl bis(4-methylbenzyl)phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂ / 1 h

2: 2-methyl-propan-2-ol

With oxalyl dichloride; In dichloromethane; tert-butyl alcohol;

Reference yield:

: 129528-98-9
bis(4-methylbenzyl)phosphine oxide

: 129529-13-1
t-butyl bis(4-methylbenzyl)phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 30percent hydrogen peroxide / methanol / 1.5 h / 90 °C

2: oxalyl chloride / CH₂Cl₂ / 1 h

3: 2-methyl-propan-2-ol

With oxalyl dichloride; dihydrogen peroxide; In methanol; dichloromethane; tert-butyl alcohol;

Reference yield:

: 104-82-5
4-Methylbenzyl chloride

: 129529-13-1
t-butyl bis(4-methylbenzyl)phosphinate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) magnesium, 2) dibutyl phosphite / 1) ether, reflux, 2) benzene, reflux, 1h

2: 75 percent / 30percent hydrogen peroxide / methanol / 1.5 h / 90 °C

3: oxalyl chloride / CH₂Cl₂ / 1 h

4: 2-methyl-propan-2-ol

With oxalyl dichloride; dibutyl hydrogen phosphite; dihydrogen peroxide; magnesium; In methanol; dichloromethane; tert-butyl alcohol;