1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzocyclopropapentalene

Base Information

• Chemical Name: 1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzo
• Molecular Formula: C₃₈H₃₀
• Molecular Weight: 486.656

Synonyms:

Chemical Property of 1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzo

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

There total 6 articles about 1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzocyclopropapentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-diphenyl-3-pentanone (5396-91-8) → 1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzocyclopropapentalene (107319-84-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) KOH; 2.) H₂SO₄ / 1.) EtOH, 40 deg C, 1 h; 2.) Ac₂O, 10 min

2: 36 percent

3: bis-(2-methoxy-ethyl) ether / Heating

4: 10 h / 240 °C

With potassium hydroxide; sulfuric acid; In diethylene glycol dimethyl ether;

Reference yield:

benzil (134-81-6) → 1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzocyclopropapentalene (107319-84-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) KOH; 2.) H₂SO₄ / 1.) EtOH, 40 deg C, 1 h; 2.) Ac₂O, 10 min

2: 36 percent

3: bis-(2-methoxy-ethyl) ether / Heating

4: 10 h / 240 °C

With potassium hydroxide; sulfuric acid; In diethylene glycol dimethyl ether;

Reference yield:

6,9-dibenzyl-7,8-diphenylbenzocyclo-octene (107337-21-3) → 1,6c-dibenzyl-2a,2b,6b,6c-terahydro-2,2a-diphenylbenzocyclopropapentalene (107319-84-6)

Guidance literature:

at 240 ℃; for 10h;

upstream raw materials:

6,9-dibenzyl-7,8-diphenylbenzocyclo-octene

bicyclo[4.2.0]octa-1,3,5,7-tetraene

1,5-diphenyl-3-pentanone

2,5-dibenzyl-3,4-diphenylcyclopenta-2,4-dienone

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