C₅₃H₇₃N₉O₁₄S₂*ClH

Base Information

Chemical Name:C₅₃H₇₃N₉O₁₄S₂*ClH
CAS No.:76314-72-2
Molecular Formula:C₅₃H₇₃N₉O₁₄S₂*ClH
Molecular Weight:1160.81
Hs Code.:

C<sub>53</sub>H<sub>73</sub>N<sub>9</sub>O<sub>14</sub>S<sub>2</sub>*ClH

Synonyms:

Suppliers and Price of C₅₃H₇₃N₉O₁₄S₂*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₇₃N₉O₁₄S₂*ClH

Chemical Property:

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Technology Process of C₅₃H₇₃N₉O₁₄S₂*ClH

There total 15 articles about C₅₃H₇₃N₉O₁₄S₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2488-15-5
N-tert-butoxycarbonyl-L-methionine

: 76314-72-2
C₅₃H₇₃N₉O₁₄S₂*ClH

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Et₃N, ethylchloroformate / 1.) THF, -10 deg C; 2.) DMF, buffer Et₃N (pH 8), 5 h

2: TFA, anisole

3: dioxane; dimethylformamide / 48 h / buffer Et₃N (pH 8)

4: 1.) TFA, anisole; 2.) 1N HCl / 2.) dioxane

With hydrogenchloride; chloroformic acid ethyl ester; methoxybenzene; triethylamine; trifluoroacetic acid; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.28.2105

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 76314-72-2
C₅₃H₇₃N₉O₁₄S₂*ClH

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / Et₃N, DCC / acetonitrile; ethyl acetate / 24 h

2: TFA, anisole / 0.5 h / Ambient temperature

3: 1.) Et₃N, ethylchloroformate / 1.) -10 deg C; 2.) THF, buffer Et₃N (pH 8), 3 h

4: hydrazine hydrate / ethanol / 12 h / Ambient temperature

5: t-butyl nitrite, 7 N HCl / dioxane; dimethylformamide / 0.17 h / -20 °C / var. reag. and time

6: dioxane; dimethylformamide / 48 h / buffer Et₃N (pH 8)

7: 1.) TFA, anisole; 2.) 1N HCl / 2.) dioxane

With hydrogenchloride; tert.-butylnitrite; chloroformic acid ethyl ester; hydrazine hydrate; methoxybenzene; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In 1,4-dioxane; ethanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.28.2105

Reference yield:

: 47510-19-0
H-Lys(Z)-Ala-OMe

: 76314-72-2
C₅₃H₇₃N₉O₁₄S₂*ClH

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Et₃N, ethylchloroformate / 1.) -10 deg C; 2.) THF, buffer Et₃N (pH 8), 3 h

2: hydrazine hydrate / ethanol / 12 h / Ambient temperature

3: t-butyl nitrite, 7 N HCl / dioxane; dimethylformamide / 0.17 h / -20 °C / var. reag. and time

4: dioxane; dimethylformamide / 48 h / buffer Et₃N (pH 8)

5: 1.) TFA, anisole; 2.) 1N HCl / 2.) dioxane

With hydrogenchloride; tert.-butylnitrite; chloroformic acid ethyl ester; hydrazine hydrate; methoxybenzene; triethylamine; trifluoroacetic acid; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.28.2105