2,2'-diphenic acid monoanilide-d₅

Base Information

• Chemical Name: 2,2'-diphenic acid monoanilide-d₅
• CAS No.: 104254-08-2
• Molecular Formula: C₂₀H₁₅NO₃
• Molecular Weight: 322.304
• Mol file: 104254-08-2.mol

Synonyms:

Chemical Property of 2,2'-diphenic acid monoanilide-d₅

Chemical Property:

Purity/Quality:

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Technology Process of 2,2'-diphenic acid monoanilide-d₅

There total 1 articles about 2,2'-diphenic acid monoanilide-d₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

biphenyl-2,2'-dicarboxylic acid anhydride (6050-13-1) + aniline-d5 (4165-61-1) → 2,2'-diphenic acid monoanilide-d5 (104254-08-2)

Guidance literature:

In xylene; at 140 - 145 ℃; for 5h; Heating;

Reference yield: 84.0%

2,2'-diphenic acid monoanilide-d5 (104254-08-2) → 6-Phenyl-d5-dibenzazepine-5,7(6H)-dione (104237-27-6)

Guidance literature:

With thionyl chloride; Heating;

upstream raw materials:

biphenyl-2,2'-dicarboxylic acid anhydride

aniline-d5

Downstream raw materials:

6-Phenyl-d₅-dibenzazepine-5,7(6H)-dione