[Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆

Base Information

Chemical Name:[Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆
CAS No.:565451-22-1
Molecular Formula:C₂₁H₁₄Cl₂N₃Pt*F₆Sb
Molecular Weight:810.089
Hs Code.:

[Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF<sub>6</sub>

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Chemical Property of [Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆

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Technology Process of [Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆

There total 1 articles about [Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 26042-64-8
silver hexafluoroantimonate

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 565451-23-2
4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine

: 565451-22-1
[Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆

Guidance literature:: In acetonitrile; byproducts: AgCl; suspn. of Pt-complex in MeCN was refluxed with AgSbF6 in MeCN for 16 h, AgCl was removed, ligand was added, refluxed for 24 h, vol. was reduced in vacuo, cooled to room temp., allowed to stand for 24 h under N2; washed with MeCN and Et2O, dried in vacuo; elem. anal.;
DOI:10.1039/b209754k

Reference yield: 89.0%

: 330660-35-0
silver cyanide

: 565451-22-1
[Pt(4'-(2'''-chlorophenyl)-2,2':6',2''-terpyridine)Cl]SbF₆

: 925204-81-5
[Pt(4'-(o-ClC₆H₄)-2,2':6',2''-terpyridine)(CN)]SbF₆

Guidance literature:: In acetonitrile; byproducts: AgCl; to suspn. Pt complex in MeCN soln. AgCN in boiling MeCN was added and heated to reflux for 24 h; soln. was filtered and concd. in vacuo, ppt. was filtered, washed with cold MeCN and dried in vacuo, extd. with hot MeCN and allowed to cool to room temp., ppt. was filtered and dried in vacuo; elem. anal.;
DOI:10.1039/b611244g