cis-[PtCl₂(PPh₂(4-veratrole))2]

Base Information

Chemical Name:cis-[PtCl₂(PPh₂(4-veratrole))2]
CAS No.:879082-72-1
Molecular Formula:C₄₀H₃₈Cl₂O₄P₂Pt
Molecular Weight:910.673
Hs Code.:

cis-[PtCl<sub>2</sub>(PPh<sub>2</sub>(4-veratrole))2]

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Chemical Property of cis-[PtCl₂(PPh₂(4-veratrole))2]

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Technology Process of cis-[PtCl₂(PPh₂(4-veratrole))2]

There total 1 articles about cis-[PtCl₂(PPh₂(4-veratrole))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 14873-63-3
cis-bis(benzonitrile)dichloroplatinum(II)

: 85417-80-7
(3,4-Dimethoxyphenyl)-diphenyl-phosphin

: 879082-72-1
cis-[PtCl₂(PPh₂(4-veratrole))2]

Guidance literature:: In dichloromethane; (under N2, Schlenk); soln. of Pt-complex in CH2Cl2 added to soln. of ligand in CH2Cl2 at room temp., stirred for 2 h; vol. reduced, MeOH added, cooled in ice, collected, washed with MeOH, dried, Et2O slow diffused, decanted, dried in vacuo;
DOI:10.1039/b513354h

Reference yield: 60.0%

: 879082-72-1
cis-[PtCl₂(PPh₂(4-veratrole))2]

: 10294-33-4
boron tribromide

: 879082-71-0
cis-[PtBr₂(PPh₂(4-catechol))2]

Guidance literature:: With HBr; KBr; In dichloromethane; (under N2, Schlenk); soln. of Pt-complex in CH2Cl2 cooled to -80°C, BBr3 added dropwise, stirred at room temp. for 3 h; volatiles removed in vacuo, MeOH added with stirring, taken to dryness in vacuo, dissolved in acetone, KBr added, stirred for 20 h, CH2Cl2, H2O,HBr added, extd., dried over Na2SO4, filtered, solvent removed in vacuo , triturated with petroleum-acetone;
DOI:10.1039/b513354h