(1S,2S,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate

Base Information

• Chemical Name: (1S,2S,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate
• CAS No.: 1153604-66-0
• Molecular Formula: C₁₉H₃₄O₃
• Molecular Weight: 310.477
• Mol file: 1153604-66-0.mol

Synonyms:

Chemical Property of (1S,2S,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,2S,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate

There total 1 articles about (1S,2S,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

syn-1-Cyclohexyl-1-hydroxy-2-methyl-3-pentanone (81640-09-7,81640-10-0,100483-71-4) + cyclohexanecarbaldehyde (2043-61-0) → (1S,2R,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate (1153604-76-2) + (1S,2S,3S)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate (1153604-66-0) + (1R,2R,3R)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate (1153604-44-4) + (1R,2S,3R)-1-cyclohexyl-3-hydroxy-2-methylpentyl cyclohexanecarboxylate (1153604-55-7)

Guidance literature:

syn-1-Cyclohexyl-1-hydroxy-2-methyl-3-pentanone; With titanium(IV) tetrabutoxide; R-BINOL; cinchonine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

cyclohexanecarbaldehyde; In dichloromethane; at 20 ℃; optical yield given as %ee; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/jo9003635

upstream raw materials:

syn-1-Cyclohexyl-1-hydroxy-2-methyl-3-pentanone

cyclohexanecarbaldehyde