C₁₄H₁₇N₃O₅

Base Information

Chemical Name:C₁₄H₁₇N₃O₅
CAS No.:1325238-19-4
Molecular Formula:C₁₄H₁₇N₃O₅
Molecular Weight:307.306
Hs Code.:

C<sub>14</sub>H<sub>17</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₁₄H₁₇N₃O₅

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Technology Process of C₁₄H₁₇N₃O₅

There total 3 articles about C₁₄H₁₇N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1325238-16-1
3-[1-(4-methoxyphenylcarbamoyl)ethylcarbamoyl]acrylic acid

: 1325238-19-4
C₁₄H₁₇N₃O₅

Guidance literature:: 3-[1-(4-methoxyphenylcarbamoyl)ethylcarbamoyl]acrylic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; for 2h; Inert atmosphere;

With O-2-tetrahydro-2H-pyranhydroxylamine; In N,N-dimethyl-formamide; at 20 ℃; for 120h; Inert atmosphere;
DOI:10.1155/2011/403129

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1325238-19-4
C₁₄H₁₇N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: diphenyl phosphoryl azide; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / 2 h / 20 °C / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4.1: lithium hydroxide / methanol; water / 2 h / 20 °C / Inert atmosphere

4.2: amberlite IRN-77

5.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide / 2 h / Inert atmosphere

5.2: 120 h / 20 °C / Inert atmosphere

With diphenyl phosphoryl azide; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1155/2011/403129

Reference yield:

: 269064-59-7
(S)-tert-butyl (1-((4-methoxyphenyl)amino)-1-oxopropan-2-yl)carbamate

: 1325238-19-4
C₁₄H₁₇N₃O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / 2 h / 20 °C / Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide / methanol; water / 2 h / 20 °C / Inert atmosphere

3.2: amberlite IRN-77

4.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide / 2 h / Inert atmosphere

4.2: 120 h / 20 °C / Inert atmosphere

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1155/2011/403129