C₂₄H₂₃Cl₂N₇O

Base Information

Chemical Name:C₂₄H₂₃Cl₂N₇O
CAS No.:1067649-41-5
Molecular Formula:C₂₄H₂₃Cl₂N₇O
Molecular Weight:496.399
Hs Code.:

C<sub>24</sub>H<sub>23</sub>Cl<sub>2</sub>N<sub>7</sub>O

Synonyms:

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Chemical Property of C₂₄H₂₃Cl₂N₇O

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Technology Process of C₂₄H₂₃Cl₂N₇O

There total 6 articles about C₂₄H₂₃Cl₂N₇O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7504-29-2
1-(2-chlorophenyl)-2-(4-chlorophenyl)ethanone

: 1067649-41-5
C₂₄H₂₃Cl₂N₇O

Guidance literature:: Multi-step reaction with 7 steps

1.1: N,N-dimethyl-formamide / 16 h / 75 °C

2.1: sodium hydride / methanol; N,N-dimethyl-formamide; mineral oil / 2.5 h / 95 °C

3.1: trichlorophosphate / 17 h / 100 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.42 h / 130 °C / Sealed microwave tube

5.1: methanesulfonic acid; water / 113 °C

6.1: trichlorophosphate / toluene / 1 h / 108 °C

7.1: hydrazine hydrate / tetrahydrofuran / 0.33 h / 20 °C

7.2: 0.58 h / 20 °C

With methanesulfonic acid; water; sodium hydride; hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 611220-83-8
6-(2-chlorophenyl)-5-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3-carbonitrile

: 1067649-41-5
C₂₄H₂₃Cl₂N₇O

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / 17 h / 100 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.42 h / 130 °C / Sealed microwave tube

3.1: methanesulfonic acid; water / 113 °C

4.1: trichlorophosphate / toluene / 1 h / 108 °C

5.1: hydrazine hydrate / tetrahydrofuran / 0.33 h / 20 °C

5.2: 0.58 h / 20 °C

With methanesulfonic acid; water; hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1065267-58-4
2-tert-butyl-7-(2-chlorophenyl)-6-(4-chlorophenyl)pyrido[2,3-d]pyrimidin-4-amine

: 1067649-41-5
C₂₄H₂₃Cl₂N₇O

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanesulfonic acid; water / 113 °C

2.1: trichlorophosphate / toluene / 1 h / 108 °C

3.1: hydrazine hydrate / tetrahydrofuran / 0.33 h / 20 °C

3.2: 0.58 h / 20 °C

With methanesulfonic acid; water; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; toluene;