(W(CO)5)3((C₆H₅)P₂(C₆H₅))

Base Information

Chemical Name:(W(CO)5)3((C₆H₅)P₂(C₆H₅))
CAS No.:98735-41-2
Molecular Formula:C₂₇H₁₀O₁₅P₂W₃
Molecular Weight:1187.86
Hs Code.:

(W(CO)5)3((C<sub>6</sub>H<sub>5</sub>)P<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>))

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Chemical Property of (W(CO)5)3((C₆H₅)P₂(C₆H₅))

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Technology Process of (W(CO)5)3((C₆H₅)P₂(C₆H₅))

There total 3 articles about (W(CO)5)3((C₆H₅)P₂(C₆H₅)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 98735-41-2
((CO)5WP(C₆H₅)P(C₆H₅)W(CO)5)W(CO)5

Guidance literature:: copper(l) chloride; In benzene; W-complex and CuCl were heated at 55°C in benzene under Ar for 3h; evapd., residue was chromd. over SiO2 (eluent hexane-toluene), crystd. from CH2Cl2; elem. anal.;
DOI:10.1021/om00131a012

Reference yield: 5.0%

: 852242-57-0
3-phenyl-3H-3-benzophosphenine pentacarbonyltungsten⁽⁰⁾

: 98735-41-2
(W(CO)5)3((C₆H₅)P₂(C₆H₅))

: [(C₁₀H₈P₂(C₆H₅)2)(W(CO)5)2]

: [(C₁₀H₈P₂(C₆H₅)2)(W(CO)5)2]

: [(C₁₀H₈P₂(C₆H₅)2)(W(CO)5)2]

: [(C₁₀H₈P₂(C₆H₅)2)(W(CO)5)2]

Guidance literature:: In toluene; (N2); at 60°C for 64 h; evapd., chromd. (SiO2, Et2O/pentane), crystd. (Et2O/pentane, -20°C);
DOI:10.1021/ja054885w

Reference yield:

: [(CH₃)2(CH₃O₂C)2C₆H₂P(C₆H₅)W(CO)5]

: W(CO)5(C₆H₅PC₂CH(CH₂)6CH)

: 98735-41-2
((CO)5WP(C₆H₅)P(C₆H₅)W(CO)5)W(CO)5

: (W(CO)5)2((C₆H₅P)2C₂CH(CH₂)6CH)

Guidance literature:: copper(l) chloride; In toluene; heating phospha(3)radialene W complex and phosphinidene precursor W complex for 3 h at 55°C in toluene with CuCl, adding extra phosphinidene precursor W complex, heating until no starting materials were detected by (31)P NMR; evapn., column chromy. (SiO2, 4:1 pentane/benzene);
DOI:10.1021/ja002437c