Technology Process of C23H16ClN5O
There total 7 articles about C23H16ClN5O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iron; ammonium chloride / ethanol; water
2: toluene-4-sulfonic acid / 1,4-dioxane / 5 h / 100 °C
With
iron; ammonium chloride; toluene-4-sulfonic acid;
In
1,4-dioxane; ethanol; water;
DOI:10.1021/ja2058583
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / dimethyl sulfoxide / 110 °C
2: iron; ammonium chloride / ethanol; water
3: toluene-4-sulfonic acid / 1,4-dioxane / 5 h / 100 °C
With
iron; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid;
In
1,4-dioxane; ethanol; water; dimethyl sulfoxide;
DOI:10.1021/ja2058583
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C
1.2: 1 h / 60 - 80 °C
2.1: boron tribromide / dichloromethane / 13 h / -78 - 20 °C / Inert atmosphere
3.1: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 3 h / 20 - 140 °C / Inert atmosphere
4.1: potassium carbonate / dimethyl sulfoxide / 110 °C
5.1: iron; ammonium chloride / ethanol; water
6.1: toluene-4-sulfonic acid / 1,4-dioxane / 5 h / 100 °C
With
hydrogenchloride; bis(triphenylphosphine)palladium(II) dichloride; boron tribromide; iron; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; triethylamine; sodium nitrite;
In
1,4-dioxane; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
3.1: Heck reaction;
DOI:10.1021/ja2058583
