C₂₆H₁₃Br₄Cl₂N₃O₂

Base Information

• Chemical Name: C₂₆H₁₃Br₄Cl₂N₃O₂
• CAS No.: 1356855-05-4
• Molecular Formula: C₂₆H₁₃Br₄Cl₂N₃O₂
• Molecular Weight: 789.93
• Mol file: 1356855-05-4.mol

Synonyms:

Chemical Property of C₂₆H₁₃Br₄Cl₂N₃O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₁₃Br₄Cl₂N₃O₂

There total 4 articles about C₂₆H₁₃Br₄Cl₂N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-dichloro-9H-carbazole (5599-71-3) → C26H13Br4Cl2N3O2 (1356855-05-4)

Guidance literature:

Multi-step reaction with 3 steps

1: nitric acid; acetic anhydride; acetic acid / 1 - 110 °C

2: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux

3: ethanol / 4 h / Reflux

With palladium on activated charcoal; nitric acid; acetic anhydride; hydrazine hydrate; acetic acid; In ethanol;

DOI:10.1016/j.inoche.2011.11.025

Reference yield:

3,6-dichloro-1,8-dinitro-9H-carbazole (104338-38-7) → C26H13Br4Cl2N3O2 (1356855-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux

2: ethanol / 4 h / Reflux

With palladium on activated charcoal; hydrazine hydrate; In ethanol;

DOI:10.1016/j.inoche.2011.11.025

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → C26H13Br4Cl2N3O2 (1356855-05-4)

Guidance literature:

Multi-step reaction with 4 steps

1: sulfuryl dichloride / dichloromethane / 4 h / 0 - 20 °C

2: nitric acid; acetic anhydride; acetic acid / 1 - 110 °C

3: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux

4: ethanol / 4 h / Reflux

With sulfuryl dichloride; palladium on activated charcoal; nitric acid; acetic anhydride; hydrazine hydrate; acetic acid; In ethanol; dichloromethane;

DOI:10.1016/j.inoche.2011.11.025

upstream raw materials:

3,5-Dibromosalicylaldehyde

1,8-diamino-3,6-dichloro-9H-carbazole

3,6-dichloro-9H-carbazole

3,6-dichloro-1,8-dinitro-9H-carbazole