Technology Process of C16H16I2N4
There total 5 articles about C16H16I2N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; hydrogenchloride / ethanol / 20 °C
2.1: methanol; sodium tetrahydroborate / tetrahydrofuran
3.1: thionyl chloride / acetonitrile / -40 °C
3.2: 20 °C
3.3: 100 °C
4.1: trifluoroacetic acid; sodium carbonate
With
hydrogenchloride; methanol; sodium tetrahydroborate; thionyl chloride; water; sodium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ja306631z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 0 - 70 °C
2.1: water; hydrogenchloride / ethanol / 20 °C
3.1: methanol; sodium tetrahydroborate / tetrahydrofuran
4.1: thionyl chloride / acetonitrile / -40 °C
4.2: 20 °C
4.3: 100 °C
5.1: trifluoroacetic acid; sodium carbonate
With
hydrogenchloride; methanol; sodium tetrahydroborate; thionyl chloride; water; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/ja306631z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methanol; sodium tetrahydroborate / tetrahydrofuran
2.1: thionyl chloride / acetonitrile / -40 °C
2.2: 20 °C
2.3: 100 °C
3.1: trifluoroacetic acid; sodium carbonate
With
methanol; sodium tetrahydroborate; thionyl chloride; sodium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; acetonitrile;
DOI:10.1021/ja306631z
