[^MeNacnacTiCl₃]

Base Information

• Chemical Name: [^MeNacnacTiCl₃]
• CAS No.: 956726-89-9
• Molecular Formula: C₂₉H₄₁Cl₃N₂Ti
• Molecular Weight: 571.897

Synonyms:

Chemical Property of [^MeNacnacTiCl₃]

Chemical Property:

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Technology Process of [^MeNacnacTiCl₃]

There total 1 articles about [^MeNacnacTiCl₃] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) + titanium tetrachloride (7550-45-0) → (HC(CMeN(2,6-(i)Pr2C6H3))2)TiCl3 (956726-89-9)

Guidance literature:

With n-BuLi; In hexane; toluene; byproducts: LiCl; under N2 atm. to ligand in toluene at -78°C n-BuLi in hexane was added, stirred at -78°C for 1 h, allowed to warm to r.t., stirred overnight, cooled to -78°C, soln. TiCl4 in toluene was added, stirred at -78°C for 2 h + 16 h at r.t.; soln. was filtered and concd., ppt. was washed with n-hexane; elem. anal.;

DOI:10.1039/b710470g

Reference yield: 80.0%

MeLi-(Et2O)0137 + [MeNacnacTiCl3] (956726-89-9) → [(HC(CMeN(2,6-(i-Pr)2C6H3))2)TiMe3] (956726-91-3)

Guidance literature:

In toluene; byproducts: LiCl; (N2); Schlenk technique; toluene was added to mixt. of Ti complex and MeLi at 0°C; stirred at 0°C for 16 h in dark; filtered; concd.; washed (hexane); elem. anal.;

DOI:10.1021/om800144v

Reference yield: 33.0%

[MeNacnacTiCl3] (956726-89-9) + 2.5C4H8O*C11H27P2Si(1-)*Li(1+) → [MeNacnacTi(Cl)(η2-P-PtBu2)]

Guidance literature:

In tetrahydrofuran; at -35 - 20 ℃; for 20h; Schlenk technique;

DOI:10.1021/acs.inorgchem.6b01929

upstream raw materials:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

titanium tetrachloride

Downstream raw materials:

(HC(CMeN(2,6-(i)Pr₂C₆H₃))2)TiMe₃

[(HC(CMeN(2,6-(i-Pr)2C₆H₃))2)TiMe₃]

[^MeNacnacTiCl₂]

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