2-Amino-3,6-dichlorothiobenzamide

Base Information

• Chemical Name: 2-Amino-3,6-dichlorothiobenzamide
• CAS No.: 74409-79-3
• Molecular Formula: C₇H₆Cl₂N₂S
• Molecular Weight: 221.11
• Mol file: 74409-79-3.mol

Synonyms:

Chemical Property of 2-Amino-3,6-dichlorothiobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Amino-3,6-dichlorothiobenzamide

There total 3 articles about 2-Amino-3,6-dichlorothiobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-Dichlor-2-amino-benzonitril (20926-15-2) → 2-Amino-3,6-dichlorothiobenzamide (74409-79-3)

Guidance literature:

With hydrogen sulfide; In ethanol;

DOI:10.1002/jhet.5570170113

Reference yield:

2-Amino-3,6-dichlorobenzamide (74396-73-9) → 2-Amino-3,6-dichlorothiobenzamide (74409-79-3)

Guidance literature:

With tetraphosphorus decasulfide; In toluene; for 4h; Heating;

DOI:10.1002/jhet.5570170113

Reference yield:

4,7-dichloroisatin (18711-13-2) → 2-Amino-3,6-dichlorothiobenzamide (74409-79-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 24.3 g / conc. H₂SO₄, NaN₃

2: 6.1 g / P₂S₅ / toluene / 4 h / Heating

With sodium azide; tetraphosphorus decasulfide; sulfuric acid; In toluene;

DOI:10.1002/jhet.5570170113

upstream raw materials:

3,6-Dichlor-2-amino-benzonitril

2-Amino-3,6-dichlorobenzamide

4,7-dichloroisatin