(η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate

Base Information

Chemical Name:(η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate
CAS No.:446281-70-5
Molecular Formula:CHCl₃*C₂₆H₂₉ClN₃PPdPtS₂
Molecular Weight:934.973
Hs Code.:

(η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate

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Chemical Property of (η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate

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Technology Process of (η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate

There total 2 articles about (η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: bis(η3-allyl-μ-chloropalladium(II))

: 67-66-3,8013-54-5
chloroform

: [(P(C₆H₅)2(C₅H₄N))ClPt(H(C₂H₅)2N₂C₂S₂)]

: 446281-70-5
(η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate

Guidance literature:: In methanol; chloroform; (Pd(C3H5)Cl)2 dissolved in CH3OH/CHCl3 (70/30), reacted with (P(C6H5)2(C5H4N))ClPt(H(C2H5)2N2S2C2 (0.5 equiv.), soln. allowed to stand for 2 h; solvent removed, dissolved in CHCl3, column chromy. (alumina, equilibrated with light petroleum), concd., pptn. by addn. of petroleum ether, recrystd. from chloroform; elem. anal.;
DOI:10.1107/S0108270102006303

Reference yield:

: 281225-74-9
[(P(C₆H₅)2(C₅H₄N))ClPt(H₂(C₂H₅)2N₂C₂S₂)]⁽¹⁺⁾*Cl^(1-)=[(P(C₆H₅)2(C₅H₄N))ClPt(H₂(C₂H₅)2N₂C₂S₂)]Cl

: 446281-70-5
(η3-allyl-2κ3-C)(chloro-1κCl)(μ-N,N'-diethyldithioxamidato-1:2κ4-S,S':N,N')[diphenyl(2-pyridyl)phosphine-1κP]palladium(II)platinum(II) chloroform solvate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium bicarbonate / chloroform

2: chloroform; methanol

With sodium bicarbonate; In methanol; chloroform;
DOI:10.1107/S0108270102006303