C₂₇H₃₁NO₃

Base Information

Chemical Name:C₂₇H₃₁NO₃
CAS No.:1420009-32-0
Molecular Formula:C₂₇H₃₁NO₃
Molecular Weight:417.548
Hs Code.:

C<sub>27</sub>H<sub>31</sub>NO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₁NO₃

Chemical Property:

Purity/Quality:

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Technology Process of C₂₇H₃₁NO₃

There total 7 articles about C₂₇H₃₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1420011-89-7
C₂₇H₃₂BrNO₃

: 1420009-32-0
C₂₇H₃₁NO₃

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis(di-tertbutylphosphino)ferrocene; triethylamine; In N,N-dimethyl-formamide; at 130 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja3121394

Reference yield:

: 104-10-9
2-(4'-aminophenyl)ethyl alcohol

: 1420009-32-0
C₂₇H₃₁NO₃

Guidance literature:: Multi-step reaction with 6 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

2: 1H-imidazole; tert-butyldimethylsilyl chloride; dmap / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 20 °C / Inert atmosphere

6: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis(di-tertbutylphosphino)ferrocene; triethylamine / N,N-dimethyl-formamide / 3 h / 130 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; 1,1'-bis(di-tertbutylphosphino)ferrocene; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 6: |Larock Annulation;
DOI:10.1021/ja3121394

Reference yield:

: C₁₄H₂₄BrNOSi

: 1420009-32-0
C₂₇H₃₁NO₃

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 20 °C / Inert atmosphere

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis(di-tertbutylphosphino)ferrocene; triethylamine / N,N-dimethyl-formamide / 3 h / 130 °C / Inert atmosphere

With pyridine; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis(di-tertbutylphosphino)ferrocene; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 4: |Larock Annulation;
DOI:10.1021/ja3121394