C₂₂H₂₈N₂O₄

Base Information

Chemical Name:C₂₂H₂₈N₂O₄
CAS No.:1431768-45-4
Molecular Formula:C₂₂H₂₈N₂O₄
Molecular Weight:384.475
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₈N₂O₄

Chemical Property:

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Technology Process of C₂₂H₂₈N₂O₄

There total 10 articles about C₂₂H₂₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₄N₂O₃*C₂HF₃O₂

: 98-88-4
benzoyl chloride

: 1431768-45-4
C₂₂H₂₈N₂O₄

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jm4002296

Reference yield:

: C₂₉H₄₁NO₃Si

: 1431768-45-4
C₂₂H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 7 h

2.1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / 7.67 h / -78 - 20 °C

3.1: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C

4.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 18.5 h / 0 - 20 °C

5.1: toluene / 13 h / Reflux

5.2: 1 h / 20 °C

6.1: triethylamine; pivaloyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

7.1: dichloromethane / 1.25 h / 0 - 20 °C

8.1: triethylamine / dichloromethane / 0 °C

With sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; pivaloyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol; 2.1: |Swern Oxidation / 5.1: |Curtius Rearrangement;
DOI:10.1021/jm4002296

Reference yield:

: C₂₄H₃₃NOSi

: 1431768-45-4
C₂₂H₂₈N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / tetrahydrofuran / 27 h / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 7 h

3.1: oxalyl dichloride; triethylamine / dichloromethane; dimethyl sulfoxide / 7.67 h / -78 - 20 °C

4.1: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2 h / 20 °C

5.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 18.5 h / 0 - 20 °C

6.1: toluene / 13 h / Reflux

6.2: 1 h / 20 °C

7.1: triethylamine; pivaloyl chloride / dichloromethane / 1.5 h / 0 - 20 °C

8.1: dichloromethane / 1.25 h / 0 - 20 °C

9.1: triethylamine / dichloromethane / 0 °C

With sodium chlorite; 2-methyl-but-2-ene; oxalyl dichloride; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; pivaloyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol; 3.1: |Swern Oxidation / 6.1: |Curtius Rearrangement;
DOI:10.1021/jm4002296