Technology Process of C23H18N2O3
There total 4 articles about C23H18N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N,N-dimethyl-aniline; trichlorophosphate / 12 h / Reflux
2: palladium diacetate; sodium carbonate; triphenylphosphine / water; 1,4-dioxane / 5 h / Reflux
With
palladium diacetate; sodium carbonate; N,N-dimethyl-aniline; triphenylphosphine; trichlorophosphate;
In
1,4-dioxane; water;
2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tetlet.2014.01.042
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / water; ethanol / 3 h / Reflux
2: nitric acid / water / 0 - 20 °C
3: N,N-dimethyl-aniline; trichlorophosphate / 12 h / Reflux
4: palladium diacetate; sodium carbonate; triphenylphosphine / water; 1,4-dioxane / 5 h / Reflux
With
hydrogenchloride; nitric acid; palladium diacetate; sodium carbonate; N,N-dimethyl-aniline; triphenylphosphine; trichlorophosphate;
In
1,4-dioxane; ethanol; water;
1: |Biginelli Pyrimidone Synthesis / 4: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tetlet.2014.01.042
- Guidance literature:
-
Multi-step reaction with 3 steps
1: nitric acid / water / 0 - 20 °C
2: N,N-dimethyl-aniline; trichlorophosphate / 12 h / Reflux
3: palladium diacetate; sodium carbonate; triphenylphosphine / water; 1,4-dioxane / 5 h / Reflux
With
nitric acid; palladium diacetate; sodium carbonate; N,N-dimethyl-aniline; triphenylphosphine; trichlorophosphate;
In
1,4-dioxane; water;
3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tetlet.2014.01.042