2--1,3-dimethyloxybenzol

Base Information

Chemical Name:2--1,3-dimethyloxybenzol
CAS No.:102861-88-1
Molecular Formula:C₁₇H₂₂O₂S₂
Molecular Weight:322.492
Hs Code.:

2-<Cyclohexyliden(vinylthio)methylthio>-1,3-dimethyloxybenzol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--1,3-dimethyloxybenzol

Chemical Property:

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Technology Process of 2--1,3-dimethyloxybenzol

There total 3 articles about 2--1,3-dimethyloxybenzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51857-29-5
2-cyclohexyliden-1,3-dithiolane

: 102861-88-1
2--1,3-dimethyloxybenzol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / MCPBA / CH₂Cl₂

2: 1.) (CF₃CO)2O, 2.) KH, / 1.) CF₃COOH, -30 deg C, 2.) THF, -78 deg C, 30 min,

With potassium hydride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1016/S0040-4039(00)95012-3

Reference yield:

: 102861-62-1
2-Cyclohexyliden-1,3-dithiolan-1-oxid

: 151-10-0
1,3-Dimethoxybenzene

: 102862-16-8
(2,4-Dimethoxyphenyl)vinylsulfid

: 102861-80-3
1,3-Dimethoxy-2-vinylsulfanyl-benzene

: 102862-07-7
4--1,3-dimethyloxybenzol

: 102861-88-1
2--1,3-dimethyloxybenzol

Guidance literature:: With potassium hydride; trifluoroacetic anhydride; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) CF₃COOH, -30 deg C, 2.) THF, -78 deg C, 30 min,;
DOI:10.1016/S0040-4039(00)95012-3