Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Base Information

Chemical Name:Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine
CAS No.:106502-59-4
Molecular Formula:C₆H₁₅N*C₅₅H₄₈N₇O₉PS
Molecular Weight:1115.26
Hs Code.:

Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Synonyms:

Suppliers and Price of Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

There total 4 articles about Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 106502-52-7
Dithiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S,S'-diphenyl ester

: 121-44-8
triethylamine

: 106502-59-4
Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Guidance literature:: With pyridine; hypophosphorous acid; for 0.166667h;
DOI:10.1021/jo00381a047

Reference yield:

: 6711-37-1
N⁶,N⁶-dibenzoyldeoxyadenosine

: 106502-59-4
Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / dimethylformamide / 0.17 h

2: mesitylenedisulfonyl chloride (MDS) / 0.17 h

3: 100 percent / phosphinic acid (PSA), pyridine / 0.17 h

With pyridine; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; hypophosphorous acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo00381a047

Reference yield:

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 106502-59-4
Thiophosphoric acid O-{(2R,3S,5R)-5-(6-dibenzoylamino-purin-9-yl)-2-[(3-imidazol-1-ylmethyl-phenyl)-bis-(4-methoxy-phenyl)-methoxymethyl]-tetrahydro-furan-3-yl} ester S-phenyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: mesitylenedisulfonyl chloride (MDS) / 0.17 h

2: 100 percent / phosphinic acid (PSA), pyridine / 0.17 h

With pyridine; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; hypophosphorous acid;
DOI:10.1021/jo00381a047