5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

Base Information

Chemical Name:5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)
CAS No.:118825-13-1
Molecular Formula:C₂₁H₂₄N₂O₄
Molecular Weight:368.433
Hs Code.:

Synonyms:

Suppliers and Price of 5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

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Chemical Property of 5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

Chemical Property:

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Technology Process of 5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

There total 8 articles about 5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38226-14-1
3-methoxy-2-methyl-6-nitrophenol

: 118825-13-1
5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / N,N-diisopropylethylamine / CH₂Cl₂

2: 96 percent / hydrogen / palladium oxide-carbon / methyl acetate / Ambient temperature

3: 1.) Cl₂, 2.) triethylamine / CH₂Cl₂

4: 68 percent / activated molecular sieve

5: lithium diisopropylamide / tetrahydrofuran

With molecular sieve; hydrogen; chlorine; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium oxide on charcoal; In tetrahydrofuran; dichloromethane; acetic acid methyl ester;
DOI:10.1039/P19880001823

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 118825-13-1
5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / sodium nitrite, sulphuric acid / H₂O

2: 64 percent / nitric acid / H₂O / Ambient temperature

3: 79 percent / potassium carbonate / acetone / 18 h

4: 95 percent / N,N-diisopropylethylamine / CH₂Cl₂

5: 96 percent / hydrogen / palladium oxide-carbon / methyl acetate / Ambient temperature

6: 1.) Cl₂, 2.) triethylamine / CH₂Cl₂

7: 68 percent / activated molecular sieve

8: lithium diisopropylamide / tetrahydrofuran

With molecular sieve; sulfuric acid; hydrogen; nitric acid; chlorine; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; sodium nitrite; palladium oxide on charcoal; In tetrahydrofuran; dichloromethane; acetic acid methyl ester; water; acetone;
DOI:10.1039/P19880001823

Reference yield:

: 65882-00-0
2-methyl-4-nitrosobenzene-1,3-diol

: 118825-13-1
5-Methoxy-7-methoxymethoxy-6-methyl-2-phenylindol-3-yl-(N,N-dimethylcarboxamide)

Guidance literature:: Multi-step reaction with 7 steps

1: 64 percent / nitric acid / H₂O / Ambient temperature

2: 79 percent / potassium carbonate / acetone / 18 h

3: 95 percent / N,N-diisopropylethylamine / CH₂Cl₂

4: 96 percent / hydrogen / palladium oxide-carbon / methyl acetate / Ambient temperature

5: 1.) Cl₂, 2.) triethylamine / CH₂Cl₂

6: 68 percent / activated molecular sieve

7: lithium diisopropylamide / tetrahydrofuran

With molecular sieve; hydrogen; nitric acid; chlorine; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium oxide on charcoal; In tetrahydrofuran; dichloromethane; acetic acid methyl ester; water; acetone;
DOI:10.1039/P19880001823