phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate

Base Information

• Chemical Name: phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate
• CAS No.: 100277-86-9
• Molecular Formula: C₁₅H₁₇O₃PS
• Molecular Weight: 308.338
• Mol file: 100277-86-9.mol

Synonyms:

Chemical Property of phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate

There total 1 articles about phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylene oxide (503-30-0) + O-phenyl phenylphosphonothioic acid (100277-95-0) → phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate (100277-86-9)

Guidance literature:

for 0.5h; Heating;

DOI:10.1007/BF01142812

Reference yield: 38.5%

phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate (100277-86-9) → 2-phenyl-2-oxo-1,3,2-thiaoxaphosphorinane + phenol (108-95-2,27073-41-2)

Guidance literature:

In xylene; for 1h; Heating;

DOI:10.1007/BF01142812

Reference yield: 35.0%

phenyl-O-phenyl-S-(3-hydroxypropyl) thiophosphonate (100277-86-9) → phenyl-O-phenyl-S-(3-chloropropyl) thiophosphonate

Guidance literature:

With phosphorus pentachloride; In dichloromethane; for 0.333333h; Heating;

DOI:10.1007/BF01142812

upstream raw materials:

trimethylene oxide

O-phenyl phenylphosphonothioic acid

Downstream raw materials:

phenol