tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate

Base Information

Chemical Name:tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate
CAS No.:1309446-25-0
Molecular Formula:C₂₆H₂₄O₄S
Molecular Weight:432.54
Hs Code.:

Synonyms:

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Chemical Property of tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate

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Technology Process of tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate

There total 2 articles about tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1044572-77-1
tert-butyl 4-[(4-methoxyphenyl)sulfinyl]benzoate

: 1309446-25-0
tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

1.2: 25 °C / Inert atmosphere

2.1: isopropylmagnesium bromide / tetrahydrofuran / 0.08 h / 60 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

2.3: 2 h / 50 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; isopropylmagnesium bromide; In tetrahydrofuran;
DOI:10.1002/chem.201003657

Reference yield:

: 31401-23-7
p-methoxybenzenesulfinyl chloride

: 1309446-25-0
tert-butyl 4-((4-methoxyphenyl)sulfinyl)-3-(phenylethynyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / -20 - 25 °C / Inert atmosphere

2.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

3.1: isopropylmagnesium bromide / tetrahydrofuran / 0.08 h / 60 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

3.3: 2 h / 50 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; isopropylmagnesium bromide; In tetrahydrofuran;
DOI:10.1002/chem.201003657