C₁₅H₁₉Cl₂NO₂

Base Information

Chemical Name:C₁₅H₁₉Cl₂NO₂
CAS No.:1314593-98-0
Molecular Formula:C₁₅H₁₉Cl₂NO₂
Molecular Weight:316.227
Hs Code.:

C<sub>15</sub>H<sub>19</sub>Cl<sub>2</sub>NO<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₉Cl₂NO₂

Chemical Property:

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Technology Process of C₁₅H₁₉Cl₂NO₂

There total 4 articles about C₁₅H₁₉Cl₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7a-(3,4-dichlorophenyl)-3H-hexahydroisobenzofuran-1-one

: 1314593-98-0
C₁₅H₁₉Cl₂NO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: ChiralTech AD column / methanol; ethanol; hexane; diethylamine / Resolution of racemate

With n-butyllithium; In tetrahydrofuran; methanol; ethanol; hexane; diethylamine;
DOI:10.1021/jm101312a

Reference yield:

: 2611-01-0
8-oxabicyclo[4,3,0]nonane-7-one

: 1314593-98-0
C₁₅H₁₉Cl₂NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tri-tert-butyl phosphine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / toluene / 0.25 h / 140 °C / Inert atmosphere; Microwave irradiation

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: ChiralTech AD column / methanol; ethanol; hexane; diethylamine / Resolution of racemate

With n-butyllithium; tri-tert-butyl phosphine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; hexane; diethylamine; toluene;
DOI:10.1021/jm101312a

Reference yield:

: 18282-59-2
4-bromo-1,2-dichlorobenzene

: 1314593-98-0
C₁₅H₁₉Cl₂NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tri-tert-butyl phosphine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / toluene / 0.25 h / 140 °C / Inert atmosphere; Microwave irradiation

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: ChiralTech AD column / methanol; ethanol; hexane; diethylamine / Resolution of racemate

With n-butyllithium; tri-tert-butyl phosphine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; hexane; diethylamine; toluene;
DOI:10.1021/jm101312a