(3-methylphenyl)cycloheptane

Base Information

• Chemical Name: (3-methylphenyl)cycloheptane
• CAS No.: 93536-65-3
• Molecular Formula: C₁₄H₂₀
• Molecular Weight: 188.313

Synonyms:

Chemical Property of (3-methylphenyl)cycloheptane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of (3-methylphenyl)cycloheptane

There total 4 articles about (3-methylphenyl)cycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-tolylmagnesium bromide (28987-79-3) → (3-methylphenyl)cycloheptane (93536-65-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i), (ii) aq. oxalic acid

2: H₂ / Pd-C

With hydrogen; palladium on activated charcoal;

DOI:10.1039/jr9630000373

Reference yield:

Cycloheptene (628-92-2,45509-99-7) + toluene (108-88-3,15644-74-3,16713-13-6) → (4-methylphenyl)cycloheptane (92298-88-9) + (2-methylphenyl)cycloheptane (92298-87-8) + (3-methylphenyl)cycloheptane (93536-65-3) + 1-methyl-1-(4-methylphenyl)cyclohexane (14962-12-0)

Guidance literature:

With toluene-4-sulfonic acid; for 6h; Heating;

DOI:10.1021/jo971832r

Reference yield:

cycloheptanol (502-41-0) + toluene (108-88-3,15644-74-3,16713-13-6) → (4-methylphenyl)cycloheptane (92298-88-9) + (2-methylphenyl)cycloheptane (92298-87-8) + (3-methylphenyl)cycloheptane (93536-65-3) + 1-methyl-1-(4-methylphenyl)cyclohexane (14962-12-0)

Guidance literature:

With sulfuric acid; at 20 ℃; for 2h; Product distribution;

upstream raw materials:

2-methyl-7,8,9,10-tetrahydro-6H-benzo[b]cyclohepta[d]thiophene

cycloheptanol

toluene

Cycloheptene

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