RuHCl(η6-C6Me6)(PPhMe2)

Base Information

Chemical Name:RuHCl(η6-C6Me6)(PPhMe2)
CAS No.:114286-49-6
Molecular Formula:C₂₀H₃₁PRu
Molecular Weight:403.51
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RuHCl(η6-C6Me6)(PPhMe2)

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Technology Process of RuHCl(η6-C6Me6)(PPhMe2)

There total 1 articles about RuHCl(η6-C6Me6)(PPhMe2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 16940-66-2
sodium tetrahydroborate

: 110800-51-6
(η(6)-C6Me6)RuCl2(dimethylphenylphosphine)

: 114286-49-6
RuHCl(η6-C6Me6)(PPhMe2)

Guidance literature:: In isopropyl alcohol; toluene; Ru-complex and NaBH4 was suspd. in propan-2-ol, the mixt. was heated under reflux for 45 min; the suspn. was evapd. to dryness under reduced pressure, the residue was extd. with toluene and the extract was filtered, under N2; toluene was pumped off and the residue was heated at 105°C/E-5 mmHg, the product being collected as powder on a probe at -20°C; elem. anal.;