NMo(OSi(C₆H₅)2C(CH₃)3)3

Base Information

Chemical Name:NMo(OSi(C₆H₅)2C(CH₃)3)3
CAS No.:1310096-08-2
Molecular Formula:C₄₈H₅₇MoNO₃Si₃
Molecular Weight:876.182
Hs Code.:

NMo(OSi(C<sub>6</sub>H<sub>5</sub>)2C(CH<sub>3</sub>)3)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of NMo(OSi(C₆H₅)2C(CH₃)3)3

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Technology Process of NMo(OSi(C₆H₅)2C(CH₃)3)3

There total 1 articles about NMo(OSi(C₆H₅)2C(CH₃)3)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 394246-98-1
[Mo(N[i-Pr](3,5-C₆H₃Me₂)3N]

: 93547-88-7
t-butyl diphenylsilanol

: 1310096-08-2
NMo(OSi(C₆H₅)2C(CH₃)3)3

Guidance literature:: In toluene; (N2, glovebox) a soln. of complex and phenol-compound in toluene was placed in a bomb flask, the flask was heated at 90°C oil bath for 10h, cooled; volatiles were removed in vac., dissolved in CH3CN, cooled to -35°C for several days, the solid was washed with cold CH3CN, dissolved in CH3CN, pptn. was repeated twice more, dissolved in C6H6, frozen, lyophilized, dried in vac., as oil;
DOI:10.1021/ic1024247