Technology Process of C25H35NO6Si
There total 4 articles about C25H35NO6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-((2-formyl-3-methylphenoxy)methyl)benzoic acid;
With
chloroformic acid ethyl ester; triethylamine;
In
tetrahydrofuran;
at 0 ℃;
for 4h;
Inert atmosphere;
3-aminopropyltriethoxysilane;
In
tetrahydrofuran;
Inert atmosphere;
DOI:10.1002/anie.201107095
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dipotassium peroxodisulfate
2.1: aluminum (III) chloride / dichloromethane / 20 °C
3.1: 18-crown-6 ether; potassium carbonate / acetone / 40 °C
4.1: methanol; sodium hydroxide / dichloromethane / 20 °C
5.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere
5.2: Inert atmosphere
With
methanol; aluminum (III) chloride; dipotassium peroxodisulfate; 18-crown-6 ether; chloroformic acid ethyl ester; potassium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1002/anie.201107095
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 18-crown-6 ether; potassium carbonate / acetone / 40 °C
2.1: methanol; sodium hydroxide / dichloromethane / 20 °C
3.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere
3.2: Inert atmosphere
With
methanol; 18-crown-6 ether; chloroformic acid ethyl ester; potassium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1002/anie.201107095
