C₂₄H₃₂F₃N₃O₄

Base Information

Chemical Name:C₂₄H₃₂F₃N₃O₄
CAS No.:1357569-97-1
Molecular Formula:C₂₄H₃₂F₃N₃O₄
Molecular Weight:483.531
Hs Code.:

C<sub>24</sub>H<sub>32</sub>F<sub>3</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₄H₃₂F₃N₃O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₃₂F₃N₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₃₂F₃N₃O₄

There total 8 articles about C₂₄H₃₂F₃N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1267597-50-1
(R)-4-isopropyl-3-((S)-2-methylpent-4-enoyl)-5,5-diphenyloxazolidin-2-one

: 1357569-97-1
C₂₄H₃₂F₃N₃O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran; hexanes / -40 - -30 °C / Inert atmosphere

1.2: 1.42 h / 0 °C / Inert atmosphere

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 24 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.2: 19 h

4.1: dmap / dichloromethane / 0 - 23 °C

5.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 23 °C

6.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide / methanol

8.1: Dess-Martin periodane

With dmap; n-butyllithium; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium bromide; In tetrahydrofuran; methanol; hexanes; dichloromethane;
DOI:10.1021/ol3000712

Reference yield:

: 1357569-95-9
benzyl (2S)-4-acetoxy-5,5,5-trifluoro-2-methylpentanoate

: 1357569-97-1
C₂₄H₃₂F₃N₃O₄

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 23 °C

2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane

3: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide / methanol

4: Dess-Martin periodane

With palladium 10% on activated carbon; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium bromide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol3000712

Reference yield:

: 152441-67-3
benzyl (S)-2-methyl-4-oxabutanoate

: 1357569-97-1
C₂₄H₃₂F₃N₃O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 19 h

2.1: dmap / dichloromethane / 0 - 23 °C

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 23 °C

4.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide / methanol

6.1: Dess-Martin periodane

With dmap; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium bromide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol3000712