C₃₂H₃₉NO₄Si

Base Information

Chemical Name:C₃₂H₃₉NO₄Si
CAS No.:1447825-84-4
Molecular Formula:C₃₂H₃₉NO₄Si
Molecular Weight:529.751
Hs Code.:

C<sub>32</sub>H<sub>39</sub>NO<sub>4</sub>Si

Synonyms:

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Chemical Property of C₃₂H₃₉NO₄Si

Chemical Property:

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Technology Process of C₃₂H₃₉NO₄Si

There total 8 articles about C₃₂H₃₉NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 251444-03-8
(1R,2S)-2-(tert-butyldiphenylsilyloxy)methyl-1-formylcyclopropane

: 1447825-84-4
C₃₂H₃₉NO₄Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

1.2: 0.33 h / 0 °C

2.1: water; hydrogenchloride / tetrahydrofuran / 1 h / 0 °C

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tert-butyl alcohol; water / 0.67 h / 20 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

5.2: 1 h / -78 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

6.2: 24 h / -78 °C

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.33 h / -78 °C

7.2: 1 h / 20 °C

8.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 1 h / 20 °C

9.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.17 h / 0 - 20 °C

With hydrogenchloride; sodium chlorite; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; water; toluene; tert-butyl alcohol; 1.1: |Wittig Olefination;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-49-1
C₂₂H₂₈O₃Si

: 1447825-84-4
C₃₂H₃₉NO₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 1 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1 h / -78 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

3.2: 24 h / -78 °C

4.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.33 h / -78 °C

4.2: 1 h / 20 °C

5.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 1 h / 20 °C

6.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.17 h / 0 - 20 °C

With sodium chlorite; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium hexamethyldisilazane; diisobutylaluminium hydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/jm400542h

Reference yield:

: C₂₃H₃₀O₂Si

: 1447825-84-4
C₃₂H₃₉NO₄Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: water; hydrogenchloride / tetrahydrofuran / 1 h / 0 °C

2.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tert-butyl alcohol; water / 0.67 h / 20 °C

3.1: triethylamine / dichloromethane / 1 h / 0 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

4.2: 1 h / -78 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

5.2: 24 h / -78 °C

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.33 h / -78 °C

6.2: 1 h / 20 °C

7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 1 h / 20 °C

8.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2.17 h / 0 - 20 °C

With hydrogenchloride; sodium chlorite; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; water; sodium hexamethyldisilazane; diisobutylaluminium hydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/jm400542h