Technology Process of C10H14N8O9P2
There total 7 articles about C10H14N8O9P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyrophosphate tetrabutylammonium salt;
In
dimethyl sulfoxide;
for 48h;
Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)92285-8
- Guidance literature:
-
Multi-step reaction with 7 steps
1: pyridine / dimethylformamide
2: Et3N / DMAP / acetonitrile / Ambient temperature
3: 2percent C6H5SO3H / CH2Cl2; methanol
4: DCC, pyridine
5: 0.4 N LiOH / 1 h
6: DCC / 2-methyl-propan-2-ol; H2O / Heating
7: tetrabutylammonium pyrophosphate / dimethylsulfoxide / 48 h
With
pyridine; lithium hydroxide; pyrophosphate tetrabutylammonium salt; triethylamine; dicyclohexyl-carbodiimide; benzenesulfonic acid;
dmap;
In
methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)92285-8
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Et3N / DMAP / acetonitrile / Ambient temperature
2: 2percent C6H5SO3H / CH2Cl2; methanol
3: DCC, pyridine
4: 0.4 N LiOH / 1 h
5: DCC / 2-methyl-propan-2-ol; H2O / Heating
6: tetrabutylammonium pyrophosphate / dimethylsulfoxide / 48 h
With
pyridine; lithium hydroxide; pyrophosphate tetrabutylammonium salt; triethylamine; dicyclohexyl-carbodiimide; benzenesulfonic acid;
dmap;
In
methanol; dichloromethane; water; dimethyl sulfoxide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)92285-8
