[(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl]

Base Information

• Chemical Name: [(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl]
• CAS No.: 1097934-03-6
• Molecular Formula: C₁₄H₁₅Cl₂N₃OPtS
• Molecular Weight: 539.345
• Mol file: 1097934-03-6.mol

Synonyms:

Chemical Property of [(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of [(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl]

There total 1 articles about [(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2-(p-chlorophenylazo)aniline + potassium tetrachloroplatinate(II) (10025-99-7) + dimethyl sulfoxide (67-68-5,8070-53-9) → [(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl] (1097934-03-6)

Guidance literature:

In dimethyl sulfoxide; soln. of 2-(p-chlorophenylazo)aniline (0.5 mmol) added to soln. of K2PtCl4 (0.5 mmol); stirred (5 h, 60°C); evapd.; chromd. (silica gel, toluene); evapd.; elem. anal.;

DOI:10.1002/ejic.200700350

Reference yield: 70.0%

[(2-(p-chlorophenylazo)aniline-H)Pt(dimethyl sulfoxide)Cl] (1097934-03-6) + acetylacetone (123-54-6,81235-32-7) → [(2-(p-chlorophenylazo)aniline-H)Pt(acetylacetone-H)] (1097934-15-0)

Guidance literature:

In methanol; acetylacetone (0.38 mmol) added to soln. of Pt complex (0.1 mmol); refluxed (4 h); evapd.; chromd. (silica gel (60-120 mesh), toluene); evapd.; elem. anal.;

DOI:10.1002/ejic.200700350

upstream raw materials:

potassium tetrachloroplatinate(II)

dimethyl sulfoxide

Downstream raw materials:

[(2-(p-chlorophenylazo)aniline-H)Pt(acetylacetone-H)]