[(C₅(C₆H₅)5)Fe(C₅H₄COCH₂CH₂COOH)]

Base Information

• Chemical Name: [(C₅(C₆H₅)5)Fe(C₅H₄COCH₂CH₂COOH)]
• CAS No.: 1291105-26-4
• Molecular Formula: C₄₄H₃₄FeO₃
• Molecular Weight: 666.599

Synonyms:

Chemical Property of [(C₅(C₆H₅)5)Fe(C₅H₄COCH₂CH₂COOH)]

Chemical Property:

Purity/Quality:

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Technology Process of [(C₅(C₆H₅)5)Fe(C₅H₄COCH₂CH₂COOH)]

There total 1 articles about [(C₅(C₆H₅)5)Fe(C₅H₄COCH₂CH₂COOH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

succinic acid anhydride (108-30-5) + (η5-C5Ph5)Fe(η5-C5H5) → [(C5(C6H5)5)Fe(C5H4COCH2CH2COOH)] (1291105-26-4)

Guidance literature:

With AlCl₃; In dichloromethane; (Ar); using Schlenk techniquus; addn. of AlCl3 and CH2Cl2 to flask, addn. dropwise of soln. of CpFe(C5Ph5) via cannula, addn. of succinic anhydride, stirring at room temp. for 24 h; cooling with ice bath, slow addn. of ice water for 5 min, sepn. of org. phase, washing with H2O, drying over Na2SO4, filtration, removal of solvent under reduced pressure, flash chromy. (SiO2, hexanes/Et2O 1/1);

DOI:10.1021/om2002206

Reference yield: 84.0%

[(C5(C6H5)5)Fe(C5H4COCH2CH2COOH)] (1291105-26-4) → [(C5(C6H5)5)Fe(C5H4CH2CH2CH2COOH)] (1291105-27-5)

Guidance literature:

With HgCl₂; Zn; HCl; In water; toluene; (Ar); using Schlenk techniquus; addn. of Zn dust and HgCl2 to (C5Me5)Fe(C5H4COCH2CH2COOH) and toluene, vigorous stirring with addn. of H2O and then HCl via syringe, reflux for 24 h; cooling to room temp., filtration, transferring of mother liquor into sepn. funnel, removal of aq. phase, washing of org. phase with brine, drying over Na2SO4, filtration, evapn. of solvent under reduced pressure, flash chromy. (SiO2, hexanes/Et2O 2/1);

DOI:10.1021/om2002206

upstream raw materials:

succinic acid anhydride

Downstream raw materials:

[(C₅(C₆H₅)5)Fe(C₅H₄CH₂CH₂CH₂COOH)]

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