cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol

Base Information

Chemical Name:cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol
CAS No.:78976-14-4
Molecular Formula:C₂₀H₂₆N₂
Molecular Weight:294.44
Hs Code.:

Synonyms:

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Chemical Property of cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol

Chemical Property:

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Technology Process of cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol

There total 6 articles about cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5787-28-0
(S)-2-phenyl-1-butane

: 78976-14-4
cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol

Guidance literature:: Multi-step reaction with 3 steps

1: 6.2 percent / 65percent HNO₃ / acetic anhydride / 1) 2 h, 0 deg C, 2) 18 h, r.t.

2: Zn, 25 percent aq. NaOH / ethanol / 1 h / 85 °C

3: 17 percent / MnO₂ / CHCl₃

With manganese(IV) oxide; sodium hydroxide; nitric acid; zinc; In ethanol; chloroform; acetic anhydride;

Reference yield:

: 4593-90-2,772-15-6
(S)-2-phenylbutanoic acid

: 78976-14-4
cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol

Guidance literature:: Multi-step reaction with 6 steps

1: LiAlH₄

2: PBr₃

3: 1) Mg, 2) H₂O

4: 6.2 percent / 65percent HNO₃ / acetic anhydride / 1) 2 h, 0 deg C, 2) 18 h, r.t.

5: Zn, 25 percent aq. NaOH / ethanol / 1 h / 85 °C

6: 17 percent / MnO₂ / CHCl₃

With manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; water; nitric acid; phosphorus tribromide; magnesium; zinc; In ethanol; chloroform; acetic anhydride;

Reference yield:

: 2031-46-1
(3S)-3-phenylbutan-1-ol

: 78976-14-4
cis-(S,S)-(-)-2,2'-Di-sec-butylazobenzol

Guidance literature:: Multi-step reaction with 5 steps

1: PBr₃

2: 1) Mg, 2) H₂O

3: 6.2 percent / 65percent HNO₃ / acetic anhydride / 1) 2 h, 0 deg C, 2) 18 h, r.t.

4: Zn, 25 percent aq. NaOH / ethanol / 1 h / 85 °C

5: 17 percent / MnO₂ / CHCl₃

With manganese(IV) oxide; sodium hydroxide; water; nitric acid; phosphorus tribromide; magnesium; zinc; In ethanol; chloroform; acetic anhydride;