N-phenylalanine methyl ester

Base Information

Chemical Name:N-phenylalanine methyl ester
CAS No.:145641-42-5
Molecular Formula:C₂₄H₃₂N₂O₅S
Molecular Weight:460.594
Hs Code.:

N-<N-(t-Butoxycarbonyl)-2(S)-benzylhypotauryl>phenylalanine methyl ester

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Suppliers and Price of N-phenylalanine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenylalanine methyl ester

Chemical Property:

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Technology Process of N-phenylalanine methyl ester

There total 7 articles about N-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 145641-39-0
((S)-1-Chlorosulfinylmethyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester

: 145641-42-5,145682-41-3
N-phenylalanine methyl ester

Guidance literature:: With 4-methyl-morpholine;
DOI:10.1016/S0040-4039(00)60981-4

Reference yield:

: 66605-57-0
(S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol

: 145641-42-5,145682-41-3
N-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / Et₃N

2: 93 percent / Cs₂CO₃ / dimethylformamide / Ambient temperature

3: Ac₂O, Cl₂ / CH₂Cl₂ / 1 h / -18 - -10 °C

4: 66 percent / N-methylmorpholine / CH₂Cl₂; dimethylformamide / Ambient temperature

With 4-methyl-morpholine; acetic anhydride; chlorine; caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00121a038

Reference yield:

: 126301-19-7,134807-64-0,109687-66-3
(2S)-2-[(tert-butoxycarbonyl)amino]-3-phenylpropyl methanesulfonate

: 145641-42-5,145682-41-3
N-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / Cs₂CO₃ / dimethylformamide / Ambient temperature

2: Ac₂O, Cl₂ / CH₂Cl₂ / 1 h / -18 - -10 °C

3: 66 percent / N-methylmorpholine / CH₂Cl₂; dimethylformamide / Ambient temperature

With 4-methyl-morpholine; acetic anhydride; chlorine; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00121a038