[Pt(CSe₃)(bis(diphenylphosphino)ferrocene)]

Base Information

• Chemical Name: [Pt(CSe₃)(bis(diphenylphosphino)ferrocene)]
• CAS No.: 785784-41-0
• Molecular Formula: C₃₅H₂₈FeP₂PtSe₃
• Molecular Weight: 998.362
• Mol file: 785784-41-0.mol

Synonyms:

Chemical Property of [Pt(CSe₃)(bis(diphenylphosphino)ferrocene)]

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of [Pt(CSe₃)(bis(diphenylphosphino)ferrocene)]

There total 1 articles about [Pt(CSe₃)(bis(diphenylphosphino)ferrocene)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

[1,1'-bis(diphenylphosphino)ferrocene]platinum(II) chloride (104413-90-3) + carbon diselenide (506-80-9) → [Pt(CSe3)(bis(diphenylphosphino)ferrocene)] (785784-41-0)

Guidance literature:

In dichloromethane; ammonia; NH3 (liquid); under N2; Pt-contg. compd. (0.122 mmol) was added to liq. NH3 (-78°C); then a soln. of CSe2 (0.265 mmol) in CH2Cl2 was added; the mixt. was stirred for 2 h at -78°C; slow warming to room temp. with stirring; the solvent was removed under reduced pressure; the residue was extd. with CH2Cl2; the mixt. was filtered, resulting soln. was reduced in vol.; Et2O was added to ppt. the compd.; elem. anal.;

DOI:10.1039/b416356g

upstream raw materials:

[1,1'-bis(diphenylphosphino)ferrocene]platinum(II) chloride

carbon diselenide