C₂₂H₂₄Br₂O₄S₂

Base Information

Chemical Name:C₂₂H₂₄Br₂O₄S₂
CAS No.:1374636-47-1
Molecular Formula:C₂₂H₂₄Br₂O₄S₂
Molecular Weight:576.37
Hs Code.:

C<sub>22</sub>H<sub>24</sub>Br<sub>2</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₄Br₂O₄S₂

Chemical Property:

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Technology Process of C₂₂H₂₄Br₂O₄S₂

There total 6 articles about C₂₂H₂₄Br₂O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261470-90-9
C₇H₃BrClIO

: 1374636-47-1
C₂₂H₂₄Br₂O₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / toluene / 12 h / -80 - 20 °C / Inert atmosphere

2.1: TurboGrignard / -80 °C / Inert atmosphere

2.2: Inert atmosphere

2.3: Inert atmosphere

With TurboGrignard; potassium tert-butylate; In toluene;
DOI:10.1002/anie.201106734

Reference yield:

: 1374636-43-7
tert-butyl 3-bromo-4-iodobenzoate

: 1374636-47-1
C₂₂H₂₄Br₂O₄S₂

Guidance literature:: tert-butyl 3-bromo-4-iodobenzoate; With TurboGrignard; at -80 ℃; Inert atmosphere;

With zinc(II) chloride; Inert atmosphere;

With disulfur dichloride; Inert atmosphere;
DOI:10.1002/anie.201106734

Reference yield:

: 249647-25-4
3-bromo-4-iodobenzoic acid

: 1374636-47-1
C₂₂H₂₄Br₂O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / toluene / 14 h / 20 °C / Inert atmosphere; Reflux

2.1: potassium tert-butylate / toluene / 12 h / -80 - 20 °C / Inert atmosphere

3.1: TurboGrignard / -80 °C / Inert atmosphere

3.2: Inert atmosphere

3.3: Inert atmosphere

With TurboGrignard; thionyl chloride; potassium tert-butylate; In toluene;
DOI:10.1002/anie.201106734