C₃₁H₃₃N₇O₃*ClH

Base Information

Chemical Name:C₃₁H₃₃N₇O₃*ClH
CAS No.:1404537-13-8
Molecular Formula:C₃₁H₃₃N₇O₃*ClH
Molecular Weight:588.109
Hs Code.:

C<sub>31</sub>H<sub>33</sub>N<sub>7</sub>O<sub>3</sub>*ClH

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₃N₇O₃*ClH

Chemical Property:

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Technology Process of C₃₁H₃₃N₇O₃*ClH

There total 22 articles about C₃₁H₃₃N₇O₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404532-70-2
{3-[4-(4-butyryl-5-methyl-pyrazol-1-yl)phenylcarbamoyl]-5-bromo-indol-1-yl}acetic acid methyl ester

: 1404537-13-8
C₃₁H₃₃N₇O₃*ClH

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 7 h / 100 °C / Inert atmosphere

2: sodium hydroxide; water / methanol

3: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / 20 °C / Alkaline conditions

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm500588w

Reference yield:

: 1404531-81-2
{3-[4-(4-butyryl-5-methyl-pyrazol-1-yl)phenylcarbamoyl]-5-cyano-indol-1-yl}acetic acid methyl ester

: 1404537-13-8
C₃₁H₃₃N₇O₃*ClH

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / methanol

2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / 20 °C / Alkaline conditions

With water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydroxide; In methanol;
DOI:10.1021/jm500588w

Reference yield:

: 10075-50-0
5-bromo-1H-indole

: 1404537-13-8
C₃₁H₃₃N₇O₃*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether / 2 h / -5 °C

2.1: potassium hydroxide / water / 4 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / -10 - 20 °C

3.2: 20 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / 1,2-dichloro-ethane / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 7 h / 100 °C / Inert atmosphere

6.1: sodium hydroxide; water / methanol

7.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / 20 °C / Alkaline conditions

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; In methanol; diethyl ether; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm500588w