C₃₃H₃₁N₃O₈

Base Information

Chemical Name:C₃₃H₃₁N₃O₈
CAS No.:1416981-55-9
Molecular Formula:C₃₃H₃₁N₃O₈
Molecular Weight:597.624
Hs Code.:

C<sub>33</sub>H<sub>31</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₁N₃O₈

Chemical Property:

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Technology Process of C₃₃H₃₁N₃O₈

There total 2 articles about C₃₃H₃₁N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39757-29-4
methyl 2,4-dioxo-4-p-tolylbutanoate

: 1416981-55-9
C₃₃H₃₁N₃O₈

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; hydrazine hydrate / 1 h / Reflux

2: hydroxylamine hydrochloride; sodium hydroxide / methanol / 1 h / 80 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

With hydroxylamine hydrochloride; benzotriazol-1-ol; hydrazine hydrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.10.099

Reference yield:

: 192701-73-8
methyl 5-(p-tolyl)-1H-pyrazole-3-carboxylate

: 1416981-55-9
C₃₃H₃₁N₃O₈

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium hydroxide / methanol / 1 h / 80 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0 - 20 °C

With hydroxylamine hydrochloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.10.099