C₂₃H₂₅F₃N₄O₂

Base Information

Chemical Name:C₂₃H₂₅F₃N₄O₂
CAS No.:1426916-04-2
Molecular Formula:C₂₃H₂₅F₃N₄O₂
Molecular Weight:446.472
Hs Code.:

C<sub>23</sub>H<sub>25</sub>F<sub>3</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₃H₂₅F₃N₄O₂

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Technology Process of C₂₃H₂₅F₃N₄O₂

There total 6 articles about C₂₃H₂₅F₃N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 372-19-0
meta-fluoroaniline

: 1426916-04-2
C₂₃H₂₅F₃N₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / water / 12 h / 0 - 20 °C

1.2: 12 h / 0 - 20 °C

2.1: acetic acid / 0.25 h / 150 °C / Microwave irradiation

2.2: 3 h / Enzymatic reaction

3.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 36 h

4.1: methanol; dichloromethane / 0.5 h / 20 °C

4.2: 24 h

5.1: hydrogenchloride / methanol; dichloromethane; 1,4-dioxane / 16 h / 20 °C

6.1: N,N-dimethyl-d₆-formamide / 20 °C / Alkaline conditions

With hydrogenchloride; palladium on activated charcoal; hydrogen; acetic acid; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-d₆-formamide;
DOI:10.1021/jm301782e

Reference yield:

: 97861-33-1
1-(3-fluorophenyl)-1,3,8-triazaspiro<4.5>decan-4-one

: 1426916-04-2
C₂₃H₂₅F₃N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; dichloromethane / 0.5 h / 20 °C

1.2: 24 h

2.1: hydrogenchloride / methanol; dichloromethane; 1,4-dioxane / 16 h / 20 °C

3.1: N,N-dimethyl-d₆-formamide / 20 °C / Alkaline conditions

With hydrogenchloride; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-d₆-formamide;
DOI:10.1021/jm301782e

Reference yield:

: 1244639-63-1
8-benzyl-1-(3-fluorophenyl)-1,3,8-triazaspiro[4.5]decan-4-one

: 1426916-04-2
C₂₃H₂₅F₃N₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; palladium on activated charcoal; hydrogen / methanol / 36 h

2.1: methanol; dichloromethane / 0.5 h / 20 °C

2.2: 24 h

3.1: hydrogenchloride / methanol; dichloromethane; 1,4-dioxane / 16 h / 20 °C

4.1: N,N-dimethyl-d₆-formamide / 20 °C / Alkaline conditions

With hydrogenchloride; palladium on activated charcoal; hydrogen; acetic acid; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-d₆-formamide;
DOI:10.1021/jm301782e