C₂₅H₃₁N₃O₄S₂

Base Information

Chemical Name:C₂₅H₃₁N₃O₄S₂
CAS No.:1623807-64-6
Molecular Formula:C₂₅H₃₁N₃O₄S₂
Molecular Weight:501.671
Hs Code.:

C<sub>25</sub>H<sub>31</sub>N<sub>3</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₅H₃₁N₃O₄S₂

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Technology Process of C₂₅H₃₁N₃O₄S₂

There total 4 articles about C₂₅H₃₁N₃O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₉N₃O₄S₂

: 1623807-64-6
C₂₅H₃₁N₃O₄S₂

Guidance literature:: With sodium cyanoborohydride; In 1,2-dichloro-ethane; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201400881

Reference yield:

: 1623807-38-4
C₁₆H₁₈N₂O₂S

: 1623807-64-6
C₂₅H₃₁N₃O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1: copper(I) thiophene-2-carboxylate / toluene / 20 °C / Schlenk technique

2: C₃₂H₆₄O₈Rh₂ / 1,2-dichloro-ethane / 2 h / 80 °C / Inert atmosphere; Schlenk technique

3: sodium cyanoborohydride / 1,2-dichloro-ethane / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With copper(I) thiophene-2-carboxylate; C₃₂H₆₄O₈Rh₂; sodium cyanoborohydride; In 1,2-dichloro-ethane; toluene;
DOI:10.1002/anie.201400881

Reference yield:

: 6719-02-4
2-(1H-pyrrol-1-yl)ethanol

: 1623807-64-6
C₂₅H₃₁N₃O₄S₂

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 24 h / 0 - 20 °C / Schlenk technique

2: copper(I) thiophene-2-carboxylate / toluene / 20 °C / Schlenk technique

3: C₃₂H₆₄O₈Rh₂ / 1,2-dichloro-ethane / 2 h / 80 °C / Inert atmosphere; Schlenk technique

4: sodium cyanoborohydride / 1,2-dichloro-ethane / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With copper(I) thiophene-2-carboxylate; di-isopropyl azodicarboxylate; C₃₂H₆₄O₈Rh₂; sodium cyanoborohydride; triphenylphosphine; In tetrahydrofuran; 1,2-dichloro-ethane; toluene;
DOI:10.1002/anie.201400881