Technology Process of C23H31NO2
There total 4 articles about C23H31NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / acetonitrile / 12 h
2: Amberlite 401 ion exchange resin / tetrahydrofuran / 4 h / Ambient temperature
With
Amberlite 401 ion exchange resin;
In
tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4020(01)88037-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / potassium carbonate / acetonitrile / Heating
2: 99 percent / NaBH4 / methanol / 1 h / Ambient temperature
3: 42 percent / oxalyl chloride, DMF / CH2Cl2 / 2 h / Heating
4: 70 percent / acetonitrile / 12 h
5: Amberlite 401 ion exchange resin / tetrahydrofuran / 4 h / Ambient temperature
With
sodium tetrahydroborate; oxalyl dichloride; Amberlite 401 ion exchange resin; potassium carbonate; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)88037-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / acetonitrile / 12 h
2: Amberlite 401 ion exchange resin / tetrahydrofuran / 4 h / Ambient temperature
With
Amberlite 401 ion exchange resin;
In
tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4020(01)88037-6