C₂₅H₂₄O₃

Base Information

• Chemical Name: C₂₅H₂₄O₃
• CAS No.: 1353219-98-3
• Molecular Formula: C₂₅H₂₄O₃
• Molecular Weight: 372.464
• Mol file: 1353219-98-3.mol

Synonyms:

Chemical Property of C₂₅H₂₄O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₄O₃

There total 3 articles about C₂₅H₂₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H18O5 + benzyl bromide (100-39-0) → C20H20O4 (1353219-97-2) + C25H24O3 (1353219-98-3)

Guidance literature:

C₁₄H₁₈O₅; With sodium ethanolate; In tetrahydrofuran; at 35 ℃; for 15h;

benzyl bromide; In tetrahydrofuran; at 35 ℃; for 48h;

DOI:10.1016/j.tetlet.2011.11.042

Reference yield:

C14H16O5 → C20H20O4 (1353219-97-2) + C25H24O3 (1353219-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogen; palladium diacetate / tetrahydrofuran / 5 h / 25 °C

2.1: sodium ethanolate / tetrahydrofuran / 15 h / 35 °C

2.2: 48 h / 35 °C

With hydrogen; sodium ethanolate; palladium diacetate; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2011.11.042

Reference yield:

4,5-dimethoxy-2-(methoxycarbonyl)benzenediazonium tetrafluoroborate → C20H20O4 (1353219-97-2) + C25H24O3 (1353219-98-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: palladium diacetate / tetrahydrofuran / 12 h / 40 °C

2.1: hydrogen; palladium diacetate / tetrahydrofuran / 5 h / 25 °C

3.1: sodium ethanolate / tetrahydrofuran / 15 h / 35 °C

3.2: 48 h / 35 °C

With hydrogen; sodium ethanolate; palladium diacetate; In tetrahydrofuran; 1.1: Heck reaction;

DOI:10.1016/j.tetlet.2011.11.042

upstream raw materials:

benzyl bromide