C₅₃H₅₃F₆N₃PtS₂

Base Information

• Chemical Name: C₅₃H₅₃F₆N₃PtS₂
• CAS No.: 1587641-04-0
• Molecular Formula: C₅₃H₅₃F₆N₃PtS₂
• Molecular Weight: 1105.23
• Mol file: 1587641-04-0.mol

Synonyms:

Chemical Property of C₅₃H₅₃F₆N₃PtS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₃H₅₃F₆N₃PtS₂

There total 5 articles about C₅₃H₅₃F₆N₃PtS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4’-bis(n-hexyl)-2,2’-bipyridine (445027-76-9) → C53H53F6N3PtS2 (1587641-04-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: diethyl ether / 12 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

1.2: 4 h / 20 °C / Schlenk technique; Inert atmosphere

2.1: acetonitrile; water / 18 h / Schlenk technique; Inert atmosphere; Reflux

3.1: triethylamine; copper(l) iodide / dichloromethane / 15 h / 30 °C / Schlenk technique; Inert atmosphere; Darkness

4.1: chloroform-d1 / 3 h / Schlenk technique; Inert atmosphere; UV-irradiation

With copper(l) iodide; triethylamine; In diethyl ether; chloroform-d1; dichloromethane; water; acetonitrile;

DOI:10.1021/ja4131615

Reference yield:

4,4'-di(n-hexyl)-6-phenyl-2,2'-bipyridine platinum chloride (1587641-01-7) → C53H53F6N3PtS2 (1587641-04-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine; copper(l) iodide / dichloromethane / 15 h / 30 °C / Schlenk technique; Inert atmosphere; Darkness

2: chloroform-d1 / 3 h / Schlenk technique; Inert atmosphere; UV-irradiation

With copper(l) iodide; triethylamine; In chloroform-d1; dichloromethane;

DOI:10.1021/ja4131615

Reference yield:

phenyllithium (591-51-5) → C53H53F6N3PtS2 (1587641-04-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: diethyl ether / 12 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

1.2: 4 h / 20 °C / Schlenk technique; Inert atmosphere

2.1: acetonitrile; water / 18 h / Schlenk technique; Inert atmosphere; Reflux

3.1: triethylamine; copper(l) iodide / dichloromethane / 15 h / 30 °C / Schlenk technique; Inert atmosphere; Darkness

4.1: chloroform-d1 / 3 h / Schlenk technique; Inert atmosphere; UV-irradiation

With copper(l) iodide; triethylamine; In diethyl ether; chloroform-d1; dichloromethane; water; acetonitrile;

DOI:10.1021/ja4131615

upstream raw materials:

phenyllithium

4,4’-bis(n-hexyl)-2,2’-bipyridine

4,4'-di(n-hexyl)-6-phenyl-2,2'-bipyridine platinum chloride

C₅₃H₅₃F₆N₃PtS₂