S-benzyl S,S-dibutyl phosphorotrithioate

Base Information

Chemical Name:S-benzyl S,S-dibutyl phosphorotrithioate
CAS No.:31173-07-6
Molecular Formula:C₁₅H₂₅OPS₃
Molecular Weight:348.535
Hs Code.:

Synonyms:

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Chemical Property of S-benzyl S,S-dibutyl phosphorotrithioate

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Technology Process of S-benzyl S,S-dibutyl phosphorotrithioate

There total 4 articles about S-benzyl S,S-dibutyl phosphorotrithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1217597-47-1
O-potassium S,S-dibutylphosphorotrithioate

: 100-44-7
benzyl chloride

: 31173-07-6
S-benzyl S,S-dibutyl phosphorotrithioate

Guidance literature:: With potassium iodide; In dimethyl sulfoxide; toluene; at 80 ℃; for 4h; Reagent/catalyst; Temperature; Schlenk technique; Green chemistry;
DOI:10.1039/d0gc02985h

Reference yield:

: 1217597-47-1
O-potassium S,S-dibutylphosphorotrithioate

: 100-39-0
benzyl bromide

: 31173-07-6
S-benzyl S,S-dibutyl phosphorotrithioate

Guidance literature:: With potassium iodide; In dimethyl sulfoxide; toluene; at 80 ℃; for 4h; Reagent/catalyst; Temperature; Schlenk technique; Green chemistry;
DOI:10.1039/d0gc02985h

Reference yield:

: 629-45-8
dibutyl disulfide

: 31173-07-6
S-benzyl S,S-dibutyl phosphorotrithioate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus; potassium hydroxide / toluene; dimethyl sulfoxide / 4 h / 80 °C / Inert atmosphere; Schlenk technique; Green chemistry

2: potassium iodide / toluene; dimethyl sulfoxide / 4 h / 80 °C / Schlenk technique; Green chemistry

With phosphorus; potassium iodide; potassium hydroxide; In dimethyl sulfoxide; toluene;
DOI:10.1039/d0gc02985h