Technology Process of tetraethyleneglycol bis(4-carboxyphenyl)ether
There total 4 articles about tetraethyleneglycol bis(4-carboxyphenyl)ether which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / tetrahydrofuran / 24 h / 20 °C / Cooling with ice
2.1: potassium carbonate; potassium iodide / butanone / 2 h / Inert atmosphere; Reflux
2.2: 16 h / Inert atmosphere; Reflux
3.1: potassium hydroxide / water; methanol / 16 h / Reflux
With
potassium carbonate; potassium iodide; potassium hydroxide;
In
tetrahydrofuran; methanol; water; butanone;
DOI:10.1021/acs.langmuir.5b03201
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate; potassium iodide / butanone / 2 h / Inert atmosphere; Reflux
1.2: 16 h / Inert atmosphere; Reflux
2.1: potassium hydroxide / water; methanol / 16 h / Reflux
With
potassium carbonate; potassium iodide; potassium hydroxide;
In
methanol; water; butanone;
DOI:10.1021/acs.langmuir.5b03201
